Category Archives: Chemistry Practicals / SPA

Chemistry Phenomenon: Chemistry Experiments in The Laboratory

All my students have heard me talked about the doing experiments in “real” laboratories as well as the life of a chemists in the laboratories. Recently, i was at one of the local university and was managed to get a few pictures of undergraduates having their practical sessions in the academic laboratory. I thought it would be beneficial to let those students that are considering to further their higher educational studies in the specialized areas of Chemistry, to have a better idea with some pictures of work in laboratories.

First picture showed students preparing their reaction inside the fume-hood (a semi-enclosed space that sucks up and out the chemical vapour that might be released into the lab). The second picture shows a common reaction vessel with chemical reaction going on.

Hope you will find these pictures interesting and stimulate & open your mind towards Chemistry.
02042008001.jpg02042008002.jpg

O Level Chemistry SPA: Color of Copper Hydroxide Vs Copper Carbonate Vs Soluble Copper Salts

Chemistry Practicals / SPA:

Recently, i received several enquiries and questions from students on the color of copper hydroxides and copper carbonates.

I understand why the confusion. This is because in the local Secondary Schools, many of the Science (Chemistry) teachers are only showing the students of the Blue Color PPT when they test for the Cu2+ cation using alkaline solution such as dilute NaOH or aqueous Ammonia Solution. The Blue Color PPT are due to the formation of insoluble Copper Hydroxide which is very distinct.

Many of students are confused and thought all Copper Salts have a Blue Color PPT. This is certainly NOT TRUE.

Summary on Color & Form of Common Copper Salts:
* Copper Hydroxide –> Insoluble Blue Color Precipitates (PPT)
* Copper Carbonate –> Insoluble Green Color Powders
* Other soluble copper salts –> Blue Color Solutions

Below is the appearance of Copper Carbonate powder:
copper-carbonate.jpg

Hope this post helps you in some ways! =)

O Level Chemistry: SPA – Qualitative Analysis

In SPA on Qualitative Analysis, the Aim in the experiment is to assess on your ability to:
–> Make observations and readings and record them in a suitable format.

With this in mind, most of the time, they will give you all kinds of unknown samples and ask you to carry out a series of tests and note down your observations. In the end, you will be prompted with more questions and eventually they will ask you to identify the unknown sample.

Question might go like this:

Description: “Sample M is a mixture of two salts, X and Y. Salt X is soluble in water. Salt Y is insoluble in water but dissolves in nitric acid.:

Procedure: “You are to separate the Sample M into X and Y. You are then to investigate the properties of X and Y by carrying out the tests below, recording your observations in a suitable format.

1 Place 3 spatulaful of Sample M in a test tube. Record the colour of Sample M. Half-fill the test tube with water and stir the tube with a glass rod for two minutes.

2 Pour the contents of the test tube into , etc………”

In your answers, the best is to “Records observations in a clear and suitable format with complete headings/statements.”

In this way, your teachers will not be able to take away marks/points from you. Remember that Statements you write must be Complete & Observations must be recorded in a clear format with headings/statements.

In Qualitative Analysis, observations should be indicated in a clear and acceptable manner:

i.e. Precipitates (acceptable) Vs. Chalky (not acceptable these days)

i.e. Effervescence is Preferred over Bubbles Seen, etc.

Hope the above Tips & Strategies on SPA is useful to you.

Hmm.. maybe i should publish a SPA-based Practical Workbook to accompany my upcoming Secret Notebook of Mole Concepts & other mini eBooks series on Chemistry?!? Let me know your thoughts. I love to hear from you. =)

O Level Chemistry: SPA – Possible Practical Questions

Several parents and students alike have asked me on the possible practical questions that can come out for the SPA examinations.

I have this to say – SPA is in fact very very simialar to the GCE O Level Practical Examinations that we had last time.  There is not much difference between the chapters/topics that we have studied for the last 10 years. Basic Chemistry is essentially Basic Chemistry. The theories does not differ that much during the 10 – 20 years period. As such, all the practicals experiments will always revolves around the few main topics and you should be aware of it.

Check out the following Practical Guidelines that are shown in the SEAB website once again:

Scientific subjects are, by their nature, experimental. It is therefore important that the candidates carry out appropriate practical work to facilitate the learning of this subject. A list of suggested practical work is provided.

1. Separation techniques including filtration, simple paper chromatography and distillation
2. Measurements of temperature based on thermometers with 1°C graduation
3. Determination of melting point and boiling point
4. Experiments involving the preparation of salts
5. Experiments involving the solubility of salts
6. Titration involving the use of a pipette, burette and an indicator such as methyl orange or screened methyl orange; full instructions and other necessary information will be given for titration other than acid/alkali and the use of other indicators
7. Identification of ions and gases as specified in the syllabus
8. Experiments involving displacement reactions
9. Tests for oxidising and reducing agents as specified in the syllabus
10. Experiments involving speed of reactions
11. Experiments involving organic substances such as polymerisation and test for saturation

This is not intended to be an exhaustive list. Reference may be made to the techniques used in these experiments in the theory papers but no detailed description of the experimental procedures will be required.

So based on the above guidelines, you can somehow make up the list of experimental set-ups that they want you to conduct.

O Level Chemistry: School-based Science Practical Assessment (SPA)

Many students have been asking me on the things that need to take note when they are doing their SPA, and how not to loose marks to their teachers that have their “eagle eyes” on them.

School-based Science Practical Assessment (SPA) is a pretty new initiative by the Singapore’s Ministry of Education (MOE) to test the students on their ability to follow procedures correctly when carrying out an experiment to test for a certain theory or concepts.

Since this is the 1st time that we are discussing on this topic on SPA, how about we take a look at the requirements & weightage of this SPA section/paper. Information below are derived directly from the Singapore Examination & Assessment Board (SEAB) website which governs the syllabus and examination standards.

School-based Science Practical Assessment (SPA):
Paper 3 (96 marks)
The School-based Science Practical Assessment (SPA) will be conducted to assess appropriate aspects of objectives C1 to C6. SPA will take place over an appropriate period that the candidates are offering the subject. The assessment of science practical skills is grouped into 3 skill sets:
* Skill set 1 – Implementing
* Skill set 2 – Analysing
* Skill set 3 – Planning
Each candidate is to be assessed only twice for each of skill sets 1 and 2 and only once for skill set 3.

Weighting and Marks Computation of the 3 Skill Sets:
The overall level of performance of each skill set (skill sets 1, 2 and 3) is the sum total of the level
of performance of each strand within the skill set.
The weighting and marks computation of the skill sets are as follows:
spa-score-table.JPG

Hope you have a better idea of how the SPA is being assessed.

O Level Chemistry: Qualitative Analysis (QA) Tips

Below is a Table that can help us to identify cations in an unknown solution. This is very important in Qualitative Analysis Tests.

Besides SPA and Practical Examinations where the following table will be provided, you will need to memorize the table in order to answer QA questions that come out for Multiple-Choice Questions as well as Structured Questions.

But no fret, it is not that difficult to memorize it. Start by looking at Cu2+, Fe2+, Fe3+ and NH4+ because they have very distinct colours changes:

  • Cu2+ –> Blue PPT
  • Fe2+ –> Green PPT
  • Fe3+ –> Reddish Brown PPT
  • NH4+ –> Gives Pungent Ammonia Gas upon heating with NaOH
    identifying-cation.jpg (Click Image to have a better view)

PS: Do print a copy and paste it at the end of your notebook if necessary.

O Level Chemistry: Tips on Solubility of Common Salts

Many students struggled whenever questions asking on solubility of salts came out in quizes and examinations.

Although it does require students to memorize the solubility of salts, there are several trends in the solubility of different salts that can assist us to memorise better.

Check out the Table of Common Salts below. I have included solubility of Hydroxides & Phosphates, which is not mentioned in most textbooks. Hope this helps. I will post more questions on solubility of salts. Do use this table to answer those questions. Stay Tuned!
table-for-salt.JPG (Click Image to see clearly)

PS: Copy, paste &print out the table above & paste it at the back of your notebook if you find it helpful.